Effect of Drying Methods on the Particle Morphology of Microcrystalline Cellulose

Abstract

Microcrystalline cellulose (MCC) is a purified partially depolymerized nonfibrous form of cellulose, a crystalline powder composed of porous particles. In this study, the drying of MCC was investigated with two different solids content MCCs by using three different drying methods: a high-velocity cyclone dryer, a spray dryer, and a fluidized bed dryer. The effects of the different drying techniques on the geometrical dimensions and morphology of the dried MCC particles and aggregates were researched. Based on the results, the dried MCC particle morphology is highly dependent on the used raw material properties as well as the liquid removal mechanism during drying. The preserving of the morphology of the raw material MCC was mostly achieved by fluidized bed drying, which facilitated MCC to dry as discrete particles with high surface area and lesser aggregation when using the MCC with 45% dry consistency as raw material. Spray drying was observed to produce small, most circular particles with the most homogenous size distributions and high velocity cyclone largest, most heterogenous and irregular shape particles and aggregates. All results have been presented as such after drying without screening.